A simple model for the SIXS beam-line at SOLEIL (surface diffraction).
Identification
Site: SOLEIL
Author: E. Farhi, A. Resta, A. Coati
Origin: SOLEIL
Date: 2023
Description
SixS (Surface Interface X-ray Scattering) is a beamline dedicated to the study
of X-ray scattering from surfaces and interfaces of hard and soft matter in
various environments in the 5-20 keV energy range. To be sensitive to the
surface all the studies are performed in grazing-incidence geometry. The
beamline is equipped with two experimental hutches, which ae dedicated to the
study of surfaces, interfaces and nano-objets prepared:
- in-situ under UHV (Ultra High Vacuum, i.e. 10-10 mbar) conditions. A
diffractometer allows to measure X-ray scattering from samples under UHV;
- in various environments (catalysis chambers, soft matter, electrochemical
cells). A diffractometer coupled with exchangeable chambers will be able to
measure X-ray scattering from sample surfaces both in vertical or horizontal
geometries.
Grazing Incidence X-ray Diffraction (GIXD), Grazing Incidence Small Angle
X-ray Scattering (GISAXS), anomalous surface X-ray scattering, X-Ray
Reflectivity (XRR), magnetic surface X-ray scattering and coherent scattering
experiments are performed on both the facilities.
In this implementation, the multipurpose diffractometer is used, with a thin
single crystal layer on top of a Si bulk.
Position | Element
---------|--------------------------------------------------------------------
0 | the U20 undulator
15 | Slit S1 2x0.7 mm^2
16.5 | a Si(111) DCM, 40x40x10 mm^3 E0=5-20 keV
26 | Mirror M1 Si coated with Pd, elliptically vertical focusing 20x350x20 mm^3 Incident angle 0.175 deg (3 mrad)
28 | Mirror M2 at 20x550x20mm^3. (tilted 45 deg exchange horz/vert components for UHV)
33 | multipurpose diffractometer
42 | UHV diffractometer (not modelled here)
Example: E0=10 Detector: mon_spl_fluo_I=3.66859e+14
Input parameters
Parameters in boldface are required;
the others are optional.
Name
Unit
Description
Default
E0
keV
Nominal energy at the Wiggler.
13
dE
keV
Energy half-bandwidth at the Wiggler
0.1
dcm_theta
deg
Rotation angle of the DCM. 0=set from energy E0
0
M1_angle
mrad
Rotation angle of M1/M2 mirrors. When left as 0, it is set automatically from E0.
3
M1_radius
m
Curvature radius of M1 mirror (Rh, 1300x100) longitudinal. Positive=mirror is focusing. 0=flat.
1400
M2_radius
m
Curvature radius of M2 mirror (Rh, 1300x100) sagittal. Positive=mirror is focusing. 0=flat.
1400
sample_coating
str
Reflection/structure data file for the single crystal thin layer coating
"Mo.lau"
sample_bulk
str
Reflection/structure data file for the single crystal bulk